PDBx:pdbx_nmr_sample_detailsType

<xsd:complexType name="pdbx_nmr_sample_detailsType">
  <xsd:annotation>
    <xsd:documentation xml:lang="en">Complete description of each NMR sample, including the solvent system used. This example was taken from the study of MCP-1 which is a dimer under the conditions studied. Three solutions with different isotope compositions were studied. <PDBx:pdbx_nmr_sample_detailsCategory> <PDBx:pdbx_nmr_sample_details solution_id="1"> <PDBx:contents>2 mM U-15N,13C, H2O 90 &#37;, D2O 10 &#37;</PDBx:contents> <PDBx:solvent_system>MCP-1</PDBx:solvent_system> </PDBx:pdbx_nmr_sample_details> <PDBx:pdbx_nmr_sample_details solution_id="2"> <PDBx:contents>1 mM U-50&#37; 15N, MCP-1 1 mM U-50&#37; 13C, H2O 90 &#37;, D2O 10 &#37;</PDBx:contents> <PDBx:solvent_system>MCP-1</PDBx:solvent_system> </PDBx:pdbx_nmr_sample_details> <PDBx:pdbx_nmr_sample_details solution_id="3"> <PDBx:contents>2 mM U-15N, H2O 90 &#37;, D2O 10 &#37;</PDBx:contents> <PDBx:solvent_system>MCP-1</PDBx:solvent_system> </PDBx:pdbx_nmr_sample_details> </PDBx:pdbx_nmr_sample_detailsCategory></xsd:documentation>
  </xsd:annotation>
  <xsd:sequence>
    <xsd:element name="pdbx_nmr_sample_details" minOccurs="0" maxOccurs="unbounded">
      <xsd:complexType>
        <xsd:all>
          <xsd:element name="contents" minOccurs="0" maxOccurs="1" nillable="true" type="xsd:string">
            <xsd:annotation>
              <xsd:documentation xml:lang="en">A complete description of each NMR sample. Include the concentration and concentration units for each component (include buffers, etc.). For each component describe the isotopic composition, including the&#37;labeling level, if known. For example: 1. Uniform (random) labeling with 15N: U-15N 2. Uniform (random) labeling with 13C, 15N at known labeling levels: U-95&#37;13C;U-98&#37;15N 3. Residue selective labeling: U-95&#37;15N-Thymine 4. Site specific labeling: 95&#37;13C-Ala18, 5. Natural abundance labeling in an otherwise uniformly labeled biomolecule is designated by NA: U-13C; NA-K,H 2mM Ribonuclease U-15N,13C; 50mM phosphate buffer NA; 90&#37;H2O, 10&#37;D2O</xsd:documentation>
            </xsd:annotation>
          </xsd:element>
          <xsd:element name="details" minOccurs="0" maxOccurs="1" nillable="true" type="xsd:string">
            <xsd:annotation>
              <xsd:documentation xml:lang="en">Brief description of the sample providing additional information not captured by other items in the category. The added glycerol was used to raise the viscosity of the solution to 1.05 poisson.</xsd:documentation>
            </xsd:annotation>
          </xsd:element>
          <xsd:element name="label" minOccurs="0" maxOccurs="1" nillable="true" type="xsd:string">
            <xsd:annotation>
              <xsd:documentation xml:lang="en">A value that uniquely identifies this sample from the other samples listed in the entry. 15N_sample</xsd:documentation>
            </xsd:annotation>
          </xsd:element>
          <xsd:element name="solvent_system" minOccurs="0" maxOccurs="1" nillable="true" type="xsd:string">
            <xsd:annotation>
              <xsd:documentation xml:lang="en">The solvent system used for this sample. 90&#37;H2O, 10&#37;D2O</xsd:documentation>
            </xsd:annotation>
          </xsd:element>
          <xsd:element name="type" minOccurs="0" maxOccurs="1" nillable="true">
            <xsd:annotation>
              <xsd:documentation xml:lang="en">A descriptive term for the sample that defines the general physical properties of the sample. bicelle</xsd:documentation>
            </xsd:annotation>
            <xsd:simpleType>
              <xsd:restriction base="xsd:string">
                <xsd:enumeration value="solution"/>
                <xsd:enumeration value="solid"/>
                <xsd:enumeration value="bicelle"/>
                <xsd:enumeration value="emulsion"/>
                <xsd:enumeration value="fiber"/>
                <xsd:enumeration value="filamentous virus"/>
                <xsd:enumeration value="gel solution"/>
                <xsd:enumeration value="gel solid"/>
                <xsd:enumeration value="liposome"/>
                <xsd:enumeration value="membrane"/>
                <xsd:enumeration value="micelle"/>
                <xsd:enumeration value="lyophilized powder"/>
                <xsd:enumeration value="oriented membrane film"/>
                <xsd:enumeration value="fibrous protein"/>
                <xsd:enumeration value="polycrystalline powder"/>
                <xsd:enumeration value="reverse micelle"/>
                <xsd:enumeration value="single crystal"/>
              </xsd:restriction>
            </xsd:simpleType>
          </xsd:element>
        </xsd:all>
        <xsd:attribute name="solution_id" use="required" type="xsd:string">
          <xsd:annotation>
            <xsd:documentation xml:lang="en">The name (number) of the sample. 1 2 3</xsd:documentation>
          </xsd:annotation>
        </xsd:attribute>
      </xsd:complexType>
    </xsd:element>
  </xsd:sequence>
</xsd:complexType>