In this section, enter information on those experiments that were used to generate constraint data. For each NMR experiment indicate which sample and which sample conditions were used for the experiment. This example was taken from the MCP-1 study. <PDBx:pdbx_nmr_exptlCategory> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="1" solution_id="3"> <PDBx:type>3D_15N-separated_NOESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="2" solution_id="1"> <PDBx:type>3D_13C-separated_NOESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="2" experiment_id="3" solution_id="1"> <PDBx:type>4D_13C/15N-separated_NOESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="4" solution_id="1"> <PDBx:type>4D_13C-separated_NOESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="5" solution_id="1"> <PDBx:type>3D_15N-separated_ROESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="6" solution_id="3"> <PDBx:type>3D_13C-separated_ROESY</PDBx:type> </PDBx:pdbx_nmr_exptl> </PDBx:pdbx_nmr_exptlCategory> |
<xsd:complexType name="pdbx_nmr_exptlType"> <xsd:annotation> <xsd:documentation xml:lang="en">In this section, enter information on those experiments that were used to generate constraint data. For each NMR experiment indicate which sample and which sample conditions were used for the experiment. This example was taken from the MCP-1 study. <PDBx:pdbx_nmr_exptlCategory> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="1" solution_id="3"> <PDBx:type>3D_15N-separated_NOESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="2" solution_id="1"> <PDBx:type>3D_13C-separated_NOESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="2" experiment_id="3" solution_id="1"> <PDBx:type>4D_13C/15N-separated_NOESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="4" solution_id="1"> <PDBx:type>4D_13C-separated_NOESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="5" solution_id="1"> <PDBx:type>3D_15N-separated_ROESY</PDBx:type> </PDBx:pdbx_nmr_exptl> <PDBx:pdbx_nmr_exptl conditions_id="1" experiment_id="6" solution_id="3"> <PDBx:type>3D_13C-separated_ROESY</PDBx:type> </PDBx:pdbx_nmr_exptl> </PDBx:pdbx_nmr_exptlCategory></xsd:documentation> </xsd:annotation> <xsd:sequence> <xsd:element name="pdbx_nmr_exptl" minOccurs="0" maxOccurs="unbounded"> <xsd:complexType> <xsd:all> <xsd:element name="sample_state" minOccurs="0" maxOccurs="1" nillable="true"> <xsd:annotation> <xsd:documentation xml:lang="en">Physical state of the sample either anisotropic or isotropic. isotropic</xsd:documentation> </xsd:annotation> <xsd:simpleType> <xsd:restriction base="xsd:string"> <xsd:enumeration value="isotropic"/> <xsd:enumeration value="anisotropic"/> </xsd:restriction> </xsd:simpleType> </xsd:element> <xsd:element name="spectrometer_id" minOccurs="0" maxOccurs="1" nillable="true" type="xsd:integer"> <xsd:annotation> <xsd:documentation xml:lang="en">Pointer to '_pdbx_nmr_spectrometer.spectrometer_id'</xsd:documentation> </xsd:annotation> </xsd:element> <xsd:element name="type" minOccurs="0" maxOccurs="1" nillable="true" type="xsd:string"> <xsd:annotation> <xsd:documentation xml:lang="en">The type of NMR experiment. 2D NOESY 3D_15N-separated_NOESY 3D_13C-separated_NOESY 4D_13C-separated_NOESY 4D_13C/15N-separated_NOESY 3D_15N-separated_ROESY 3D_13C-separated_ROESY HNCA-J HNHA DQF-COSY P-COSY PE-COSY E-COSY</xsd:documentation> </xsd:annotation> </xsd:element> </xsd:all> <xsd:attribute name="conditions_id" use="required" type="xsd:string"> <xsd:annotation> <xsd:documentation xml:lang="en">The number to identify the set of sample conditions. 1 2 3</xsd:documentation> </xsd:annotation> </xsd:attribute> <xsd:attribute name="experiment_id" use="required" type="xsd:string"> <xsd:annotation> <xsd:documentation xml:lang="en">A numerical ID for each experiment. 1 2 3</xsd:documentation> </xsd:annotation> </xsd:attribute> <xsd:attribute name="solution_id" use="required" type="xsd:string"> <xsd:annotation> <xsd:documentation xml:lang="en">The solution_id from the Experimental Sample to identify the sample that these conditions refer to. [Remember to save the entries here before returning to the Experimental Sample form] 1 2 3</xsd:documentation> </xsd:annotation> </xsd:attribute> </xsd:complexType> </xsd:element> </xsd:sequence> </xsd:complexType> |