<xsd:complexType name="pdbx_exptl_pdType">
<xsd:annotation>
<xsd:documentation xml:lang="en">Data items in the pdbx_exptl_pd record information about powder sample preparations.</xsd:documentation>
</xsd:annotation>
<xsd:sequence>
<xsd:element name="pdbx_exptl_pd" minOccurs="0" maxOccurs="unbounded">
<xsd:complexType>
<xsd:all>
<xsd:element name="spec_preparation" minOccurs="0" maxOccurs="1" nillable="true" type="xsd:string">
<xsd:annotation>
<xsd:documentation xml:lang="en">A description of preparation steps for producing the diffraction specimen from the sample. Include any procedures related to grinding, sieving, spray drying, etc. POLYCRYSTAL SLURRY wet grinding in acetone sieved through a 44 micron (325 mesh/inch) sieve spray dried in water with 1%clay</xsd:documentation>
</xsd:annotation>
</xsd:element>
<xsd:element name="spec_preparation_pH" minOccurs="0" maxOccurs="1" nillable="true">
<xsd:annotation>
<xsd:documentation xml:lang="en">The pH at which the powder sample was prepared.</xsd:documentation>
</xsd:annotation>
<xsd:simpleType>
<xsd:restriction base="xsd:decimal">
<xsd:minInclusive value="0.0"/>
</xsd:restriction>
</xsd:simpleType>
</xsd:element>
<xsd:element name="spec_preparation_pH_range" minOccurs="0" maxOccurs="1" nillable="true" type="xsd:string">
<xsd:annotation>
<xsd:documentation xml:lang="en">The range of pH values at which the sample was prepared. Used when a point estimate of pH is not appropriate. 5.6 - 6.4</xsd:documentation>
</xsd:annotation>
</xsd:element>
</xsd:all>
<xsd:attribute name="entry_id" use="required" type="xsd:string">
<xsd:annotation>
<xsd:documentation xml:lang="en">The value of attribute entry_id in category pdbx_exptl_pd uniquely identifies a record in the PDBX_EXPTL_PD category.</xsd:documentation>
</xsd:annotation>
</xsd:attribute>
</xsd:complexType>
</xsd:element>
</xsd:sequence>
</xsd:complexType> |